E – 07 Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Atomic Emission Spectrometry, aluminum, aluminum alloys, atomic. Buy ASTM E TEST METHOD FOR ANALYSIS OF ALUMINUM AND ALUMINUM ALLOYS BY SPARK ATOMIC EMISSION. ASTM E Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Spark Atomic Emission Spectrometry Scope
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Calculate and enter appropriate correction factors in accordance with Practice E Argon also may be introduced around the counter electrode, but the ow rate shall not conne the discharge to an area less than 5 mm in diameter, to provide adequate sampling of the specimen.
Other forms may be analyzed, provided that 1 they are sufficiently massive to prevent undue heating, 2 they permit machining at surfaces having a minimum diameter of approximately 15 mm, and 3 reference materials of similar metallurgical condition and chemical composition are available.
Concentration or concentration ratio plots can be employed. Active view current version of standard. Accurate analysis of Hg using this technique is compromised by the presence of an intense iron interference. The specimen serves as one electrode, the cathode. The lines listed have proven satisfactory for the elements and concentration ranges prescribed in the Scope.
The excitation chamber shall be designed so that it can be ushed automatically with argon gas.
E12511 Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Current edition approved Jan. F1251, high-speed analysis of aluminum, before it is poured from the furnace, can prevent scrapped heats and minimize the cost of expensive alloying metals.
It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Even with this compensation for variability in background, alloys with highly different compositions of major alloying e1521, particularly silicon, require separate reference materials and analytical curves. Calibration may require only 5 to 20 calibrants. NOTE 6—A magnesium furnace is not acceptable because it will introduce variable magnesium contamination.
It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. I The detection limit for iron is determined more by possible segregation in the specimen and by contamination during machining than by spectrochemical sensitivity. For unknown specimens where usually two burns are used, this means at least four burns of the standardants.
Satm system shall include: Link to Active This link will always route to the wstm Active version of the standard. A ow gage is required to check the ow rates. These have been found to give comparable analytical performance.
NOTE 4—The background equivalents and detection limits listed in Table 1 can be attained with a reciprocal linear dispersion of 5. It can be applied to other types of specimens if there are appropriate reference materials, or if the specimens are remelted. Note 5 NOTE 5—The gain and zero controls can be omitted if the analytical program is restricted to a few alloy types, the concentration ranges in each are restricted, axtm the gain and background levels do not vary widely from day to day.
These reference materials can be used for establishing an analytical curve, but will not reveal potential interferences from nearby ee1251 of other elements, or matrix effects that change the background or response. The radiant asym of selected analytical lines and an internal standard line are converted into electrical currents by photomultipliers.
It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. This, in turn, may produce concentration readings for silicon that are too high by 0. The aluminum specimen to be analyzed may be in the form of a chill cast disk, casting, foil, sheet, plate, extrusion, or some other wrought form or shape.
See Practice E for precautions to be used in handling gases. Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM Headquarters. Two types of standardization are commonly used, as follows 3. The data are based on ten successive readings. A bad burn will have shallow pittings, surrounded by a whitish or silvery ring. The currents are integrated during the exposure time either by charging integrating capacitors and measuring the cumulative voltages at the end of the exposure, or by interrogating the capacitors during the exposure and converting the voltages into digital counts by means of a computer.
Mercury Hg is intentionally not included in the scope. Department of Commerce, Gaithersburg, MD Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
ASTM E1251 – 17a
Specific safety and health statements are given in Section Normally standardization will require ten to fteen minutes. Signicance and Use 5. Use one of the sets of electrical parameters given in Table 2.